This high-pressure reactor is ideally suitable for larger experimental runs. This high-pressure reactor is available in stainless steel 1.4571 (SUS 316LTI), Hastelloy C-22, or with PTFE lining on all sides.
The usable volume of the reactor can be varied between 4,700 ml and 5,500 ml with or without the PTFE lining.
The BR 4000 high-pressure reactor is notable for its ease of handling. The reactor is closed using quick closure chain that can be attached without the use of tools. The reactor seal is established using a conical flange lock and O-ring seal of PTFE, FKM, or FFKM. The appropriate fitting inserts are available in stainless steel 1.4571 (SUS 316LTI) or Hastelloy C-22. A total of 6 connection options are provided in the lid, which can be selected from the following:
* Immersion tube for temperature probes
* Rupture disc of metal for the safe limitation of maximum pressure
* Pressure display
* Vent valve
* 2 freely selectable fittings, for example for a gas sampling valve or liquid sampling point
Temperature is regulated using a temperature probe which detects the inner temperature of the reactor in an immersion tube. A second temperature probe can optionally be used as an independent overheating safety. Appropriate stand systems are available.
Features
* 4700, 5500 ml / 150 bar / 230℃
* Quick closure chain, to be operated manually without tools
* O-Seal ring made of Viton®, PTFE or Kalrez®
* Either with PTFE-insert or completely made of SUS 316LTi or Hastelloy®
* Heating by elctrical or thermostated mantle
* Stiring by magnetic clutch and separate drive
* Mounted on a laboratory cart for easy operation
* Optionally internal heating/cooling coil
* Optionally 2’nd thermocouple
6 Connections
* Dip-tube for thermocouple
* Rupture disc
* Pressure gauge or sensor
* Vent valve
* 2x optionally for liquid sampling, gas sampling ….
Technical Specification
| BR-4000 | |||
| Material | SUS316Ti or HC | SUS316Ti PTFE | |
| Temperature max. | 300℃ | 230℃ | |
| Pressure max. | 150 bar | ||
| Reactor Vessel | Volume | approx. 5,500 ml | |
| Inner Diameter | 136mm | ||
| Inner Height | 390mm | ||
| Weight | approx. 10.5 kg | ||
| TFMTM-PTFE Insert* (integrated) | Volume | – | approx. 4,700 ml* |
| Inner Diameter | – | 126mm | |
| Inner Height | – | 378mm | |
| Armatures | Standard Armatures | Rupture Disc, Dip Tube, Valve, Tool | |
| Pressure Measurement | analog and/or digital | ||
| Ports (total) | 6 | ||
| Ports (free) | 2** | ||
| Type of connection | 8 mm Tube Connection | ||
| Heating Systems (optional) | Electrical Heating mantle | CHM-4000 | |
| Julabo thermostat | CTM-4000 | ||
| Heating Coil | √ | ||
| Stirring | Overhead stirrer with magnetic clutch | WB18D and RV 100-SS | |
| Stand | Electric lifting stand for BR-1000 | ||
* When using PTFE inserts the maximum allowable temperature is 230℃
* The number of free ports can be enlarged by the use of T-connections
